A-A-20091D
TABLE I. Analytical data (continued)
Types
Requirements I and II III IV V
Stability, Oil Stability Index at 1100C (OSI), minimum 1/ |
5 hours |
8 hours |
8 hours |
5 hours |
Linolenic acid (percent by weight), maximum 3/ |
- |
1.5 |
3.5 |
- |
Iodine value |
- |
- |
105-120 |
- |
Insoluble impurities, maximum |
None |
None |
None |
None |
AOCS Cold Test (5.5 hours minimum) |
Pass 4/ |
Pass |
Pass |
4/ |
Moisture and volatile matter (percent by weight), maximum |
0.06 |
0.06 |
0.06 |
0.06 |
1/ Determination shall be made within seven days after packaging. Samples submitted for testing shall be in a completely filled container.
2/ Maximum of 0.06 percent free fatty acid will be acceptable if propyl gallate is added as an antioxidant.
3/ Determined by gas chromatography of methyl esters of fatty acids.
4/ Cold test is not required for peanut oil or soybean oils.
6.2 Product verification. When USDA verification of analytical requirements is specified in the solicitation, contract, or purchase order, the following procedures will be followed. Analytical testing shall be performed on a composite sample. The composite sample shall be 454 grams (1 pound) and prepared from subsamples drawn from randomly selected containers. The number of subsamples used to create the composite shall be based on USDA procedures.
6.3 Analytical testing. When specified in the solicitation, contract, or purchase order, the analyses shall be in accordance with the following methods from the Official Methods of the AOCS.
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